MIL-STD-202G
METHOD 107G
THERMAL SHOCK
1.PURPOSE. This test is conducted for the purpose of determining the resistance of a part to exposures at extremes of high and low temperatures, and to the shock of alternate exposures to these extremes, such as would be experienced when equipment or parts are transferred to and from heated shelters in arctic areas. These conditions may also be encountered in equipment operated noncontinuously in low-temperature areas or during transportation. Although it is preferred that the specimen reach thermal stability during the exposure specified, in the interest of saving time, parts may be tested at the minimum exposure durations specified, which will not insure thermal stability but only an approach thereto. Permanent changes in operating characteristics and physical damage produced during thermal shock result principally from variations in dimensions and other physical properties. Effects of thermal shock include cracking and delamination of finishes, cracking and crazing of embedding and encapsulating compounds, opening of thermal seals and case seams, leakage of filling materials, rupturing, or cracking of hermetic seals and vacuum glass to metal seals, and changes in electrical characteristics due to mechanical displacement or rupture of conductors or of insulating materials.
2.APPARATUS. Suitable temperature controlled systems shall be used to meet the temperature requirements and test conditions specified in table 107-I or table 107-III. The liquid method is more severe and may damage some components that might not be degraded by the air method. It is not intended for use on nonhermetically sealed components.
2.1Environmental chambers. A system of sufficient thermal capacity shall be used to change ambient chamber conditions to meet test requirements and to reach specified temperature conditions of steps 1 and 3 of table 107-I. The supply air temperature of the chambers shall reach the specified temperature within a recovery time of 5 minutes after the specimens have been transferred to the appropriate chamber.
2.2Liquid baths. Suitable temperature controlled baths containing liquids (see table 107-IV) shall be chosen to maintain the specified test conditions (see table 107-III) within the indicated tolerances. A liquid media shall not be used without prior approval of the qualifying activity.
3. PROCEDURE.
3.1 Environmental chambers. Specimens shall be placed so that there is substantially no obstruction to the flow of air across and around the specimen. When special mounting is required, it shall be specified. The specimen shall be subjected to the specified test condition of table 107-I. The first five cycles shall be run continuously. After five cycles, the test may be interrupted after the completion of any full cycle, and the specimens allowed to return to room ambient temperature before testing is resumed. One cycle consists of steps 1 through 4 of the applicable test condition. Specimens shall not be subjected to forced circulating air while being transferred from one chamber to another. Whether single or multiple chambers are used, the effective total transfer time from the specified low temperature to the specified high temperature, or the reverse, shall not exceed 5 minutes. Direct heat conduction to the specimen should be minimized. In the case of multiple chambers, the transfer time shall be defined as the time between withdrawal from the low temperature chamber and introduction into the high temperature chamber or the reverse.
NOTE: In single compartment chambers, in which the temperature extremes of steps 1 and 3 are achieved without physical movement of the specimens, steps 2 and 4 are not applicable.
METHOD 107G
28 March 1984
1 of 5
MIL-STD-202G
3.2 Liquid baths. Specimens shall be immersed in a suitable liquid that shall be approved by the qualifying activity (see table 107-IV), at the temperature in step 1 of the specified test condition (see table 107-III) for the time specified in table 107-V. Immediately upon the conclusion of step 1, the device shall be transferred to a suitable liquid at the temperature specified in step 2 of the specified test condition. The device shall remain at the high temperature for the time specified in table 107-V. These two steps, step 1 and 2, constitute one cycle of the applicable test condition. Repeat the required number of cycles without interruption as specified in table 107-III. Transfer time from low to high temperature and from high to low temperature shall be less than 10 seconds.
TABLE 107-I. Thermal shock test conditions (air).
|
Test |
Number of |
|
Test |
Number of |
|
Test |
Number of |
|
condition |
cycles |
|
condition |
cycles |
|
condition |
cycles |
Step |
A |
5 |
|
B |
5 |
|
C |
5 |
|
A-1 |
25 |
|
B-1 |
25 |
|
C-1 |
25 |
|
A-2 |
50 |
|
B-2 |
50 |
|
C-2 |
50 |
|
A-3 |
100 |
|
B-3 |
100 |
|
C-3 |
100 |
|
Temperature |
Time |
|
Temperature |
Time |
|
Temperature |
Time |
|
°C |
|
|
°C |
|
|
°C |
|
1 |
-55 +0, -3 |
See table |
|
-65 +0, -5 |
See table |
|
-65 +0, -5 |
See table |
|
|
107-II |
|
|
107-II |
|
|
107-II |
2 |
25 +10, -5 |
5 minutes |
|
25 +10, -5 |
5 minutes |
|
25 +10, -5 |
5 minutes |
3 |
85 +3, -0 |
maximum |
|
125 +3, -0 |
maximum |
|
200 +5, -0 |
maximum |
See table |
|
See table |
|
See table |
||||
|
|
107-II |
|
|
107-II |
|
|
107-II |
4 |
25 +10, -5 |
5 minutes |
|
25 +10, -5 |
5 minutes |
|
25 +10, -5 |
5 minutes |
|
|
maximum |
|
|
maximum |
|
|
maximum |
|
|
|
|
|
|
|
|
|
|
Test |
Number of |
|
Test |
Number of |
|
Test |
Number of |
|
condition |
cycles |
|
condition |
cycles |
|
condition |
cycles |
Step |
D |
5 |
|
E |
5 |
|
F |
5 |
|
D-1 |
25 |
|
E-1 |
25 |
|
F-1 |
25 |
|
D-2 |
50 |
|
E-2 |
50 |
|
F-2 |
50 |
|
D-3 |
100 |
|
E-3 |
100 |
|
F-3 |
100 |
|
Temperature |
Time |
|
Temperature |
Time |
|
Temperature |
Time |
|
°C |
|
|
°C |
|
|
°C |
|
1 |
-65 +0, -5 |
See table |
|
-65 +0, -5 |
See table |
|
-65 +0, -5 |
See table |
2 |
25 +10, -5 |
107-II |
|
25 +10, -5 |
107-II |
|
25 +10, -5 |
107-II |
5 minutes |
|
5 minutes |
|
5 minutes |
||||
3 |
350 +5, -0 |
maximum |
|
500 +5, -0 |
maximum |
|
150 +3, -0 |
maximum |
See table |
|
See table |
|
See table |
||||
4 |
25 +10, -5 |
107-II |
|
25 +10, -5 |
107-II |
|
25 +10, -5 |
107-II |
5 minutes |
|
5 minutes |
|
5 minutes |
||||
|
|
maximum |
|
|
maximum |
|
|
maximum |
METHOD 107G
28 March 1984
2
MIL-STD-202G
TABLE 107-II. Exposure time in air at temperature extremes.
Weight of specimen |
Minimum time |
|
(for steps 1 and 3) |
|
Hours |
1 ounce (28 grams and below) |
1/4 (or as specified) |
Above 1 ounce (28 grams) to .3 pound (136 grams), inclusive |
½ |
Above .3 pounds (136 grams) to 3 pounds (1.36 kilograms), inclusive |
1 |
Above 3 pounds (1.36 kilograms) to 30 pounds (13.6 kilograms), inclusive |
2 |
Above 30 pounds (13.6 kilograms) to 300 pounds (136 kilograms), inclusive |
4 |
Above 300 pounds (136 kilograms) |
8 |
TABLE 107-III. Thermal shock conditions (liquid).
|
Test |
Number |
|
Test |
Number |
|
Test |
Number |
|
Test |
Number |
|
condition |
of cycles |
|
condition |
of cycles |
|
condition |
of cycles |
|
condition |
of cycles |
Step |
AA |
5 |
|
BB |
5 |
|
CC |
5 |
|
DD |
5 |
|
AA-1 |
15 |
|
BB-1 |
15 |
|
CC-1 |
15 |
|
DD-1 |
15 |
|
AA-2 |
25 |
|
BB-2 |
25 |
|
CC-2 |
25 |
|
DD-2 |
25 |
|
Temperature |
Time |
|
Temperature |
Time |
|
Temperature |
Time |
|
Temperature |
Time |
|
°C |
|
|
°C |
|
|
°C |
|
|
°C |
|
1 |
-0 +2, -10 |
See table |
|
-65 +0, -10 |
See table |
|
-65 +0, -10 |
See table |
|
-65 +0, -10 |
See table |
|
|
107-V |
|
|
107-V |
|
|
107-V |
|
|
107-V |
2 |
100 +10, -2 |
See table |
|
125 +10, -0 |
See table |
|
150 +10, -0 |
See table |
|
200 +10, -0 |
See table |
|
|
107-V |
|
|
107-V |
|
|
107-V |
|
|
107-V |
METHOD 107G
28 March 1984
3
MIL-STD-202G
TABLE 107-IV. Suggested thermal fluids. 1/ 2/
Test |
AA, AA-1, AA-2 |
BB, BB-1, BB-2 |
CC, CC-1, CC-2 |
DD, DD-1, DD-2 |
||||
condition |
fluids |
Fluids |
|
fluids |
|
fluids |
|
|
Step 1 |
FC40 4/ |
or |
FC77 4/ |
|
FC77 4/ |
|
FC77 4/ |
|
|
Water 3/ |
|
|
|
|
|
|
|
|
D02 |
6/ |
D02 |
6/ |
D02 |
6/ |
D02 |
6/ |
|
D02-TS |
D02-TS |
D02-TS |
D02-TS |
||||
|
D/80 |
|
D/80 |
|
D/80 |
|
D/80 |
|
Step 2 |
FC40 4/ |
|
FC70 |
|
FC70 |
|
FC70 4/ |
|
|
Water 3/ |
|
FC40 |
4/ |
FC40 |
4/ |
|
|
|
|
|
UCON-WS 5/ |
UCON-WS 5/ |
UCON-WS} 5/ |
|||
|
D02 |
|
D02 |
|
D02 |
|
D05 |
|
|
D02-TS |
6/ |
D02-TS |
6/ |
D02-TS |
6/ |
LS/230 |
6/ |
|
D03 |
|
D03 |
|
D03 |
|
LS/215 |
|
1/ See 2.2.
2/ Ethylene glycol shall not be used as a thermal shock test fluid.
3/ Tap water is indicated as an acceptable fluid for this temperature range. Its suitability chemically shall be established prior to use. A mixture of water and alcohol may be used to prevent freezing at the low temperature extreme. The water shall not be allowed to boil at the upper temperature extreme.
4/ FC77, FC70, FC40 are the registered trademark of 3M.
5/ UCON-WS process fluid is the registered trademark of Union Carbide Corporation.
6/ D02, D02-TS, D03, D05, D/80, LS/215 and LS/230 are the registered trademark of Ausimont (Division of Montedison).
TABLE 107-V. Exposure time in liquid at temperature extremes.
Weight of specimen |
Minimum time |
|
(for steps 1 and 2) |
.05 ounce (1.4 grams) and below |
½ |
Above .05 ounce (1.4 grams) to .5 ounce (14 grams) |
2 |
Above .5 ounce (14 grams) to 5 ounces (140 grams) |
5 |
METHOD 107G
28 March 1984
4
MIL-STD-202G
4.MEASUREMENTS. Specified measurements shall be made prior to the first cycle and upon completion of the final cycle, except that failures shall be based on measurements made after the specimen has stabilized at room temperature following the final cycle.
5.SUMMARY. The following details are to be specified in the individual specification:
a.Recovery time if other than 5 minutes (see 2.1).
b.Special mounting, if applicable (see 3).
c.Type test (air or liquid) and test condition (see 3).
d.Transfer time if other than specified in 3.1 or 3.2.
e.Measurements before and after cycling (see 4).
METHOD 107G
28 March 1984
5